By Stefan Mathias Sarge, G?nther W. H. H?hne, Wolfgang Hemminger
Essentially divided into 3 components, this sensible booklet starts via facing all primary elements of calorimetry. the second one half seems on the gear used and new advancements. The 3rd and ultimate part offers size instructions with a purpose to receive the easiest effects.
the result's optimized wisdom for clients of this method, supplemented with useful assistance and tricks.
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Extra resources for Calorimetry: Fundamentals, Instrumentation and Applications
Platinum resistance thermometers (Pt-100 thermometers) are usually made with a resistance of 100 V at 273 K. The resistance values are tabulated as a function of temperature and can be approximated by a second-order polynomial, the Callendar equation (Callendar, 1887). The manufacturers generally indicate the extent to which the Pt-100 sensor corresponds to the standard. 5 K in a range up to 250 C can usually be obtained without a subsequent calibration; more accurate measurements require either a recalibration or the use of a calibrated, and accordingly more expensive, sensor.
Acta, 20, 65–79. Robison, J. , William Creech, Edinburgh. Ter Minassian, L. and Milliou, F. (1983) An isothermal calorimeter with pneumatic compensation – principles and application. J. Phys. E: Sci. , 16, 450–455. € ber die von Steinwehr, H. (1901) Studien u Thermochemie sehr verd€ unnter L€osungen. Z. Phys. , 38, 185–199. C. (1781) Om eldens speciﬁca myckenhet uti fasta kroppar, och des afm€atande. Kongl. Swenska Wetensk. Acad. , II, 49–78. 19 2 Measuring Instruments Various calorimeters are described in Chapter 1.
Lavoisier, A. L. -S. (1784) Memoire sur la chaleur. Mem. Acad. Sci. Année 1780, 355–408. Ramsay, W. , Constable, London. Regenass, W. (1977) Thermoanalytische Methoden in der chemischen Verfahrensentwicklung. Thermochim. Acta, 20, 65–79. Robison, J. , William Creech, Edinburgh. Ter Minassian, L. and Milliou, F. (1983) An isothermal calorimeter with pneumatic compensation – principles and application. J. Phys. E: Sci. , 16, 450–455. € ber die von Steinwehr, H. (1901) Studien u Thermochemie sehr verd€ unnter L€osungen.