Caged Compounds by Gerard Marriott (Eds.)

By Gerard Marriott (Eds.)

The severely acclaimed laboratory common for greater than 40 years, Methods in Enzymology is without doubt one of the such a lot hugely revered guides within the box of biochemistry. considering that 1955, every one quantity has been eagerly awaited, usually consulted, and praised by way of researchers and reviewers alike. greater than 285 volumes were released (all of them nonetheless in print) and masses of the cloth is correct even today--truly a vital booklet for researchers in all fields of lifestyles sciences

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After filtration, the filtrate is evaporated in vacuo. The resulting viscous liquid is loaded on 5 g of DEAE-Sephadex (A-50-120; Sigma, St. Louis, MO) pretreated with 10 mM of ammonium acetate. 20 M solution to obtain the product). 2 M ammonium acetate. 2%) of p-hydroxyphenacyl diammonium phosphate (16). 18, IR (KBr) 3350, 3088, 2950, 1679, 1594, 1570, 1440, 1268, 1090 cm-1; UV-vis (CH3CN/H20) Ama~(e)220 (8400), 282 (14,000). 68; N, 10,52. 33. Coupling of p-Hydroxyphenacyl Phosphate with ADP p-Hydroxyphenacyl Adenosine 5'-Triphosphate, Triammonium Salt (17).

33. Coupling of p-Hydroxyphenacyl Phosphate with ADP p-Hydroxyphenacyl Adenosine 5'-Triphosphate, Triammonium Salt (17). 27 The coupling reaction is modeled after the method of Hoard and Ott. , Phillipsburg, NJ) (10 g) in a sintered glass funnel is treated with 5% hydrochloric acid (20 ml x 2) and washed with water until the filtrate is neutral. The resin is then treated with 20% aqueous pyridine solution and washed with water until the filtrate is neutral. A solution of adenosine 5'-diphosphate (ADP, potassium salt, 39 C.

Chem. , 18-20 (1955). 37(a) M. Kulbaand A. Zwierzak,Ann. Soc. Chim. Polonorum48,1603(1974);(b) A. Zwierzak and M. Kulba, Tetrahedron22, 3163-3170 (1971);and (c) E. P. Serebryakov,L. M. Suslova, and V. F. Kucherov, Tetrahedron34, 345-351 (1978). 5)] is stirred for 2 hr. Evaporation of acetone and H20 on a Rotavapor gives a concentrated aqueous solution of the salt. 66. 70 mmol), and 20 ml of benzene is placed in a 50-ml round-bottom flask and refluxed with efficient stirring for 10 hr. The solution is cooled to room temperature and extracted with the HzO/ethyl acetate solution.

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